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Research groups

Research Group on Nanoporous Materials

Head: prof. dr hab. inż. Andrzej B. Jarzębski

Staff

  1. prof. dr hab. inż. Andrzej B. Jarzębski
  2. dr Janusz J. Malinowski
  3. Katarzyna Maresz
  4. dr Julita Mrowiec-Białoń
  5. Aleksandra Zawadzka

Description:

  • Synthesis and characterization of nanomaterials
    • Aerogels and low-density xerogels
    • Mesoporous molecular sieves (monoliths and powders)
    • Mesoporous cellular foams for application as specific catalysts and adsorbents
    • Materials with multimodal hierarchical structure
    • Immobilization of biologically active species including enzymes in nanostructures
  • Microreactors
  • Supercritical drying and extraction with supercritical carbon dioxide

Apparatus:

  • ASAP 2020 automatic adsorption/chemisorption analyzer (Micromeritics)
  • ASAP 2000 automatic nitrogen adsorption analyzer (Micromeritics)
  • spectrofotometer FTIR NIcolet 6700 with thermobalance STAR 850 (Mettler Toledo)
  • gas pycnometer AccuPyc 1330 (Micromeritics)
  • mercury porosimeter AutoPOre II (Micromeritics)
  • microwave reactor (Plazmatronica)
  • spray dryer B-191 (Buchi)
  • high pressure reactor (Berghof)
  • HPLC (Waters) and GC (Hewlett Packard) chromatographs

    • Research networks and organisations:

    FP6 Network of Excellence INSIDE-PORES (satellite partner)

    Main achievments:

    • Synthesis of new nanoporous materials for selective sorption and catalysis/biocatalysis (patents: PL 186154, PL 175386 , RU Patent 2196764 ). They meet the objectives set for “green” chemical technologies.

    Publications

    1. Very stable silica-gel-bound laccase biocatalysts for the selective oxidation
      A. Rekuc, J. Bryjak, K. Szymańska, A. B. Jarzębski
      Biores. Technol., 101 , 2076-2083 (2010)

    2. New mesoporous materials for selective sorption and catalysis
      J. Mrowiec-Białoń,
      Annual Report PAS, 54-56 (2009)

    3. Structure studies on nanocrystalline powder of MgO xerogel prepared by sol-gel method
      G. Dercz, K. Prusik, L. Paj±k, R. Pielaszek, J.J. Malinowski, W. Pudło
      Mater. Sci. Poland, 27 , 201-207 (2009)

    4. Immobilization of invertase on mesoporous silicas to obtain hyper active biocatalysts
      K. Szymańska, J. Bryjak, A. B. Jarzębski
      Top. Catal., 52 , 1030-1036 (2009)

    5. Nanocrystalline MgO powder materials prepared by sol-gel studied by X-ray diffraction and electron microscopy
      G. Dercz, L. Paj±k, K. Prusik, R. Pielaszek, J.J. Malinowski
      Z. Kristallogr., Suppl. 30 , 255-260 (2009)

    6. Laccase immobilization on mesostructured cellular foams affords preparations with ultra high activity
      A. Rekuć, J. Bryjak, K.Szymańska, A.B. Jarzębski
      Process Biochem., 44 , 191-198 (2009)

    7. Nb-containing mesoporous materials of MCF type-Acidic and oxidative properties
      M. Trejda, J. Kujawa, M. Ziolek, J. Mrowiec-Białoń
      Cat. Today, 139 , 196-201 (2008)

    8. Fabrication and properties of silica monoliths with ultra large mesopores
      J. Mrowiec-Białoń, A.B. Jarzębski
      Micropor. Mesopor. Mater. , 109 , 429-435 (2008)

    9. Organosulfonic acid functionalised silica mesostructured cellular foams - efficient acidic catalysts for reactions of esterification
      J. Mrowiec-Białoń, K. Maresz, J.J. Malinowski, A.B. Jarzębski
      Chem. Proc. Eng., 29 , 701-711 (2008)

    10. Structure analysis of nanocrystalline MgO aerogel prepared by sol-gel method
      G. Dercz, L. Paj±k, K. Prusik, R. Pielaszek, J.J. Malinowski, W. Pudło
      Solid State Phenom., 130 , 203-206 (2007)

    11. Characterisation of nanoporous aluminosilicate monoliths derivatised with metal cations for selective propene-propane adsorption
      M. Kargol, J. Zajac, D.J. Jones., J. Roziere, A.B. Jarzębski
      Stud. Surf. Sci. Catal., 160 , 357-364 (2007)

    12. Covalent immobilization of trypsin on to siliceous mesostructured cellular foams to obtain effective biocatalysts
      K. Szymańska, J. Bryjak, J. Mrowiec-Białoń, A.B. Jarzębski
      Cat. Today, 124 , 2-10 (2007)

    13. Application and properties of siliceous mesostructured cellular foams as enzyme carriers to obtained efficient biocatalysts
      K. Szymańska, J. Bryjak, J. Mrowiec-Białoń, A. Jarzębski
      Micropor. Mesopor. Mater., 99 , 167-175 (2007)

    14. Ellipsometric study of porosity distribution in hybrid silica-based sol-gel films
      L. Więcław-Solny, A. Kudła, J. Mrowiec-Białoń, A.B. Jarzębski
      Stud. Surf. Sci. Catal., 160 , 463-469 (2007)

    15. Aerobic oxidation of α-pinene over cobalt-substituted polyoxometalate supported on amino-modified mesoporous silicates
      N.V. Maksimchuk, M.S. Melgunov, Yu.A. Chesalov, J. Mrowiec-Białoń, A. Jarzębski, O. A. Kholdeeva
      J. Catal., 246 , 241-248 (2007)

    16. Amino functinalized low density silica xerogels seen by different characterization methods
      J.Mrowiec-Białoń
      Stud. Surf. Sci. Catal., 160 , 343-350 (2007)

    17. Effect of silica-type sol-gel carrier’s structure and morphology on a supported Ziegler-Natta catalysts for ethylene polymerization
      Ł. Korach, K. Czaja, J. Mrowiec-Białoń, A. Jarzębski
      Eur. Polym. J., 42 , 3085-3092 (2006)

    18. Silica gel based composite adsorbents for water vapor
      A. B. Jarzębski, J. Mrowiec-Białoń
      Encyclopedia of Surface and Colloid Science, Taylor & Francis, 5577-5589, (2006)

    19. Fabrication of Nafion and heteropoly acid-containing thin catalytic films without failure
      L. Więcław-Solny, A. B. Jarzębski, J. Mrowiec-Białoń, W. Turek, Z. Ujma, A. Kudła, M. Gibas, J. Żak
      Appl. Catal. A: General., 285 , 79-85 (2006)

    20. Determination of hydroxyls density in the silica-mesostructured cellular foams by thermogravimetry
      J. Mrowiec-Białoń
      Thermochimica Acta, 443 , 49-52 (2006)

    21. Materials with multimodal hierarchical porosity
      W. Pudło, W. Gawlik, J. Mrowiec-Białoń, T. Buczek, J.J. Malinowski, A.B. Jarzębski
      Inż. Chem. Proces., 27 , 177-185 (2006)

    22. SAXS from particle and disordered systems
      L. Paj±k, B. Bierska-Piech, J. Mrowiec-Białoń, A.B. Jarzębski, R. Diduszko
      Fibers and Textiles in Eastern Europe, 13 , 69-74 (2005)

    23. New materials for sorption and catalysis
      A.B. Jarzębski, J. Mrowiec-Białoń, M. Kargol
      Przem. Chem., 6 , 410-414 (2005)

    24. H2O2-based allylic oxidation of α-pinene over different single site catalysts
      N.V. Maksimczuk, M.S. Melgunov, J. Mrowiec-Białoń, A.B. Jarzębski, O.A. Kholdeeva
      J. Catal., 235 , 175-183 (2005)

    25. FTIR spectroscopic study of titanium-containing mesoporous silicate materials
      N.N. Trukhan, A.A. Panchenko, E. Roduner, M.S. Mel’gunov, O.A. Kholdeeva, J. Mrowiec-Białoń, A.B. Jarzębski
      Langmuir, 21 , 10545-1055 (2005)

    26. Preparation and surface properties of low-density gels synthesized using prepolymerized silica precursors
      J. Mrowiec-Białoń, A. B. Jarzębski,, L. Paj±k, Z. Olejniczak, M. Gibas
      Langmuir, 20 , 10389-1939 (2004)

    27. Isomerization of allyl aryl ethers to their 1-propenyl derivatives catalysed by ruthenium complexes
      S. Krompiec, N. KuĽnik, R. Penczek, J. Rzepa, J. Mrowiec-Białoń
      J. Mol. Catal. A-Chem., 219 , 29-40 (2004)

    28. Properties of the Sol-Gel TiO2-SiO2 Oxidation Catalysts Prepared Using Ethyl Silicate 40 as a Silica Precursor
      J. Mrowiec-Białoń, A.B. Jarzębski, O.A. Kholdeeva, N.N. Trukhan, V.I. Zaikovski, V.V. Kriventsov, Z. Olejniczak,
      Appl.Catal. A, 273 , 47-53 (2004)

    29. Nanostructured materials obtained by sol-gel method
      A. Jarzębski, J. Mrowiec-Białoń, M. Kargol, L. Więcław-Solny
      Inż. Chem. Proc., 25 , 239-249 (2004)

    30. New nanostructured materiales for effective sorption and catalysis
      A.B. Jarzębski, J. Mrowiec-Białoń, M. Kargol
      Annual Report, Polish Academy of Sciences, 60-61 (2004)

    31. Co-containing polyoxometalate-base heterogenenous catalysts for the selective aerobic oxidation of aldehydes under ambient conditions
      O.A. Kholdeeva, M.P. Vanina, M.N. Timofeeva, R.I. Maksimovskaya, T.A. Trubitsina, M.S. Melgunov, E.B. Burgina, J. Mrowiec-Białoń, A.B. Jarzębski, C.L. Hill
      J. Catal., 226 , 363-371 (2004)

    32. Hybrid silica microparticles containing biologically active substance obtained by the sol-gel and spray drying method
      A.I. Lachowski, J, Raczek, M. Sosada, B. Pasker, A.B. Jarzębski
      Inż. Chem. Proces. , 25 , 1255 (2004)

    33. Highly selective isomerization of N-allylamides and N-allylamines
      S. Krompiec, M. Pigulla, M. Krompiec, S. Baj, J. Mrowiec-Białoń, J. Kasperczyk
      Tetrahedron Lett., 45 , 5257-5261 (2004)


    34. L. Więcław-Solny, A. B. Jarzębski, A. Kudła, J. Mrowiec-Białoń
      Inż. Chem. Proces., 25 , 1777-1782 (2004)


    35. R. Pawełczyk, K. Maresz
      Inż. Chem. Proc., 25 , 1455-1460 (2004)


    36. J. Mrowiec-Białoń, K. Szymańska, K. Maresz
      Inż. Chem. Proces., 25 , 1367-1372 (2004)


    37. R. Pawełczyk, K. Maresz,
      Inż. Aparat. Chem., 1 , 10-13 (2004)

    38. The effective approach for recovery of methyl-substituted 1,3-dioxane from aqueous media
      J.J. Malinowski, A.J. Daugulis
      Separ. Sci. Technol., 37 , 2659-2667 (2002)

    39. Two-phase partitioning bioreactors in fermentation technology
      J. Malinowski,
      Biotechnol. Adv., 19 , 525-538 (2001)

    40. Reactive extraction for downstream separation of 1,3-propanediol
      J. Malinowski,
      Biotechnol. Prog., 16 , 76-79 (2000)

    41. Enzymatic reactions in supercritical CO2
      A. Jarzębski, J. Malinowski,
      Biotechnologia, 1(44) , 238-246 (1999)


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